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By Jordan Brandes

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Viscosity may also be correlated with other, more difficult to measure properties such as molecular-weight distribution. This chapter starts with a presentation of the basic equations used to calculate viscosity, the limitations of their assumptions, and the procedures used to correct for these problems. A basic capillary rheometer is described, and then a detailed description of the steps used to set up and run an experiment is presented. Methods of interpreting the data and some procedures to gather data other than viscosity curves are also discussed.

The most common test is ASTM D671, in which a specially designed test specimen is subjected to cantilever oscillation at 30 Hz with a constant amplitude of force mode: the specimen sees the same maximum force during the test and will continue to deflect to larger and larger strains as it weakens, until failure occurs. This is in contrast to a constant-deflection fatigue test in which the sample is subject to the same maximum deflection while the resultant force is reduced asymptotically with increasing cycles.

It can be used for a wide range of elements, from sodium to uranium, and provides detection limits at the sub-parts-per-million level; it can also measure concentrations of up to 100% easily and simultaneously. ED-XRF is highly versatile and is available in a wide range configurations, from small benchtop instruments for special tasks to multipurpose laboratory spectrometers. Typical uses include the analysis of oils and fuel, plastic, rubber and textiles, pharmaceutical products, heat-resistant materials, glass, ceramics and wafers; the determination of coatings on paper, film, polyester, and metals; and the sorting of metal alloys, glass, and plastic according to their constituent materials.

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Contract Manufacturing and Packaging November-December 2011 by Jordan Brandes

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